Synthesis and characterization of reduced graphene oxidation from corn cob waste
DOI:
https://doi.org/10.24114/jpkim.v14i3.39348Abstract
Graphene is the latest carbon-based nanomaterial with wide applications and has superiority in electrical, thermal, and high conductivity properties. This study aims to synthesize and characterize reduced graphene oxide (rGO) from corncob waste using the modified Hummer method. which was carried out by removing the NaNo3 material. This synthesis used corncob waste that was made into charcoal with a particle size of 100 mesh with an oxidation time of 5 days. Structural analysis of rGO used Fourier Transform Infa Red (FTIR) and X-ray diffraction (XRD) testing. The results of FTIR testing showed a wave peak at 1568.82 cm-1 with C=C bonds which indicated that rGO was formed. The XRD test results showed a diffractogram peak at an angle of 2θ ~ 24.6635 which is typical of rGO materials.Keywords: Corncob waste; Graphene; Graphite; Modified hummer; rGOReferences
Amaia, Z. E., & Beatriz A. R. (2018). Patent Number: 3070053B1. European Patent. Madrid.
Cooper, D. R., D'Anjou, B., Ghattamaneni, N., Harack, B., Hilke, M., Horth, A., Majlis, N., Massicotte, M., Vandsburger, L., Whiteway, E., & Yu, V. (2012). Experimental Review of Graphene. ISRN Condens. Matter Phys, 2012, 501686. https://doi.org/10.5402/2012/501686
Habte, A. T., & Ayele, D. W. (2019). Synthesis and characterization of reduced graphene oxide (rGO) started from graphene oxide (GO) using the tour method with different parameters. Advances in Materials Science and Engineering, 2019, 5058163. https://doi.org/10.1155/2019/5058163
Hummers Jr, W. S., & Offeman, R. E. (1958). Preparation of graphitic oxide. Journal of the american chemical society, 80(6), 1339-1339. https://doi.org/10.1021/ja01539a017
Krishnamoorthy, K., Veeravandian, R., Mohan, R., & Kim, S-J. (2012). Investigation of Raman and photoluminescence studies of reduced graphene oxide sheets. Applied Physcs A, 106, 501-506. https://doi.org/10.1007/s00339-011-6720-6
Pei, S., & Cheng, H. M. (2012). The reduction of graphene oxide. Carbon, 50(9), 3210-3228. https://doi.org/10.1016/j.carbon.2011.11.010
Russo, P., Hu, A., & Compagnini, G. (2013). Synthesis, properties and potenial aplications of porous graphene: A review. Nano-Micro Letters, 5(4), 260-273. https://doi.org/10.1007/BF03353757
Setiadji, S., Nuryadin, B. W., Ramadhan, H., Sundari, C. D. D., Sudiarti, T., Supriadin, A., & Ivansyah, A. L. (2018). Preparation of reduced Graphene Oxide (rGO) assisted by microwave irradiation and hydrothermal for reduction methods. IOP Conf. Ser.: Mater. Sci. Eng, 434, p. 012079. https://doi.org/10.1088/1757-899X/434/1/012079
Selvakumar, N., Pradhan, U., Krupanidhi, S.B., & Barshilia, H. C. (2016). Structural and optical properties of graphene oxide prepared by modified hummers™ method. Computers, Materials and Continua, 52(3), 173-184. https://doi.org/10.3970/cmc.2016.052.173.html
Wang, X., & Dou, W. (2012). Preparation of graphite oxide (GO) and the thermal stability of silicone rubber/GO nanocomposites. Thermochimica Acta, 529, 25-28. https://doi.org/10.1016/j.tca.2011.11.016
Downloads
Published
Issue
Section
License
Copyright (c) 2022 Dyah Suci Perwitasari, Adinata Shafi Wahyudi Suwarno, Muhammad Nauli Rizqi Akbar

This work is licensed under a Creative Commons Attribution 4.0 International License.
Authors published in this journal agree to the following terms:
- The copyright of each article is retained by the author (s).
- The author grants the journal the first publication rights with the work simultaneously licensed under the Creative Commons Attribution License, allowing others to share the work with an acknowledgment of authorship and the initial publication in this journal.
- Authors may enter into separate additional contractual agreements for the non-exclusive distribution of published journal versions of the work (for example, posting them to institutional repositories or publishing them in a book), with acknowledgment of their initial publication in this journal.
- Authors are permitted and encouraged to post their work online (For example in the Institutional Repository or on their website) before and during the submission process, as this can lead to productive exchanges, as well as earlier and larger citations of published work.
Jurnal Pendidikan Kimia is licensed under a Creative Commons Attribution 4.0 International License